Microscale Organic Laboratory: WITH Multistep and Multiscale Syntheses by Dana W. Mayo
This is a laboratory text for the mainstream organic chemistry course taught at both two and four year schools, featuring both microscale experiments and options for scaling up appropriate experiments. It provides complete coverage of organic laboratory experiments and techniques with a strong emphasis on modern laboratory instrumentation, a sharp focus on safety in the lab, excellent pre- and post-lab exercises, and multi-step experiments. There is also another text available by the same authors titled Microscale Techniques for the Organic Lab, Second Edition which has more material on techniques and spectroscopy, but has no experiments.